ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE

Base Information

• Chemical Name: ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE
• CAS No.: 144632-97-3
• Molecular Formula: C12H10 F6 O2
• Molecular Weight: 300.201
• Hs Code.: 2918300090
• Mol file: 144632-97-3.mol

Synonyms:ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE;3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE;3,5-BIS(TRIFLUOROMETHYL)PHENYLACETIC ACID ETHYL ESTER;Ethyl 3,5-Bis(trifluoromethyl)phenyl acetate 97%;Ethyl3,5-Bis(trifluoromethyl)phenylacetate97%

Chemical Property of ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE

Chemical Property:

• Refractive Index: 1.4170
• Boiling Point: 219.8°Cat760mmHg
• Flash Point: 61.3°C
• PSA: 26.30000
• Density: 1.329g/cm³
• LogP: 3.82980

Purity/Quality:

97% ^*data from raw suppliers

3,5-Bis(Trifluoromethyl)phenylaceticAcidEthylEster ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE

There total 2 articles about ETHYL 3,5-BIS(TRIFLUOROMETHYL)PHENYL ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

ethanol (64-17-5) + 3,5-bistrifluoromethylphenyl acetic acid (85068-33-3) → ethyl 2-(3,5-bis(trifluoromethyl)phenyl)acetate (144632-97-3)

Guidance literature:

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃;

Reference yield: 42.5%

ethyl α-bromo-(3,5-bistrifluoromethylphenyl)acetate → ethyl 2-(3,5-bis(trifluoromethyl)phenyl)acetate (144632-97-3) + meso-diethyl 2,3-di<3,5-bis(trifluoromethyl)phenyl>succinate + DL-diethyl 2,3-di<3,5-bis(trifluoromethyl)phenyl>succinate

Guidance literature:

With tetraethylammonium perchlorate; In N,N-dimethyl-formamide; Ambient temperature; electrolysis, reticulated vitreous carbon cathode;

Reference yield: 100.0%

3-(tetrahydro-2H-pyran-2-yloxy)propyl bromide (33821-94-2) + ethyl 2-(3,5-bis(trifluoromethyl)phenyl)acetate (144632-97-3) → ethyl 2-(3,5-bis(trifluoromethyl)phenyl)-5-((tetrahydro-2H-pyran-2-yl)oxy)pentanoate

Guidance literature:

ethyl 2-(3,5-bis(trifluoromethyl)phenyl)acetate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.666667h;

3-(tetrahydro-2H-pyran-2-yloxy)propyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

upstream raw materials:

ethanol

3,5-bistrifluoromethylphenyl acetic acid

Downstream raw materials:

4-(3,5-bis-trifluoromethyl-phenyl)-2H-isoxazol-5-one

ethyl 2-(3,5-bis(trifluoromethyl)phenyl)-2-diazoacetate

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