Technology Process of C17H27NO4
There total 7 articles about C17H27NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; water; tert-butyl alcohol;
at 0 - 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: n-butyllithium / tetrahydrofuran / -78 °C
1.2: -78 - 20 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C
2.2: -78 - 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C
4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C
5.1: hydrazine hydrate / ethanol / 3 h / Heating; Reflux
6.1: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h
7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C
With
osmium(VIII) oxide; lithium aluminium tetrahydride; n-butyllithium; sodium hydrogencarbonate; hydrazine hydrate; 4-methylmorpholine N-oxide; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C
1.2: -78 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C
3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C
4.1: hydrazine hydrate / ethanol / 3 h / Heating; Reflux
5.1: sodium hydrogencarbonate / 1,4-dioxane; water / 5 h
6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 16 h / 0 - 20 °C
With
osmium(VIII) oxide; lithium aluminium tetrahydride; sodium hydrogencarbonate; hydrazine hydrate; 4-methylmorpholine N-oxide; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; tert-butyl alcohol;