(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

Base Information

Chemical Name:(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride
CAS No.:351-96-2
Molecular Formula:C₈H₆FNO₄S
Molecular Weight:231.204
Hs Code.:

Synonyms:(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

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Technology Process of (E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

There total 5 articles about (E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (Z)-2-(4-nitrophenyl)ethenesulfonyl fluoride

: 351-96-2
(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; for 0.5h; Temperature; Sealed tube;
DOI:10.1002/ejoc.201900799

Reference yield: 86.0%

: 677-25-8
ethylenesulfonyl fluoride

: 24067-17-2
4-nitrophenylboronic acid

: 351-96-2
(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

Guidance literature:: With palladium diacetate; silver nitrate; In acetic acid; at 80 ℃; for 12h; stereoselective reaction;
DOI:10.1002/adsc.201700688

Reference yield: 83.0%

: 100-13-0
4-nitrostyrene

: 351-96-2
(E)-2-(4-nitrophenyl)ethene-1-sulfonyl fluoride

Guidance literature:: With [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; fluorosulfonylchloride; In diethyl ether; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1002/anie.202012229