N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

Base Information

Chemical Name:N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide
CAS No.:1346936-32-0
Molecular Formula:Br*C₁₇H₃₀BN₂O₄
Molecular Weight:417.151
Hs Code.:

Synonyms:N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

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Chemical Property of N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

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Technology Process of N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

There total 1 articles about N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 105-59-9
N-Methyldiethanolamine

: 138500-85-3
4-bromomethylphenylboronic acid pinacol ester

: 1346936-32-0
N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1021/ja2073824

Reference yield: 70.0%

: 1346936-32-0
N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

: 1346936-29-5
N,N-bis(2-chloroethyl)-N-methyl-N-(4-boronophenyl)methanaminium bromide

Guidance literature:: With thionyl chloride; at 20 ℃;
DOI:10.1021/ja2073824

Reference yield:

: 1346936-32-0
N,N-bis(2-hydroxyethyl)-N-methyl-N-[4-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl]methanaminium bromide

: 51-75-2
nitrogen mustard

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 20 °C

2: dihydrogen peroxide / water-d2 / 2 h / pH 7.5 / aq. phosphate buffer

With thionyl chloride; dihydrogen peroxide; In water-d2;
DOI:10.1021/ja2073824