2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

Base Information

Chemical Name:2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester
CAS No.:693784-39-3
Molecular Formula:C₂₂H₂₄O₇
Molecular Weight:400.428
Hs Code.:

Synonyms:2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

Suppliers and Price of 2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

There total 1 articles about 2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 93092-16-1
5-(benzyloxy)-2,3-dimethoxybenzaldehyde

: 77924-28-8
4-tert-butyl 1-ethyl 2-(diethoxyphosphoryl)succinate

: 693784-39-3
2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

Guidance literature:: 5-(benzyloxy)-2,3-dimethoxybenzaldehyde; 4-tert-butyl 1-ethyl 2-(diethoxyphosphoryl)succinate; With sodium hydride; In tetrahydrofuran; at 20 ℃;

With trifluoroacetic acid; In water; at 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2003.11.120

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 693784-39-3
2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

: 693784-40-6
4-acetoxy-5-benzyloxy-7,8-dimethoxy-naphthalene-2-carboxylic acid ethyl ester

Guidance literature:: With potassium acetate; Heating;
DOI:10.1016/j.tetlet.2003.11.120

Reference yield:

: 693784-39-3
2-[1-(5-Benzyloxy-2,3-dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid 1-ethyl ester

: 693784-41-7
8-benzyloxy-3-hydroxymethyl-5,6-dimethoxy-1-naphthol

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / KOAc / Heating

2: K₂CO₃ / ethanol / 20 °C

3: LiAlH₄ / tetrahydrofuran / 20 °C

With lithium aluminium tetrahydride; potassium acetate; potassium carbonate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.tetlet.2003.11.120