C₁₇H₂₄OSSi

Base Information

• Chemical Name: C₁₇H₂₄OSSi
• CAS No.: 959399-22-5
• Molecular Formula: C₁₇H₂₄OSSi
• Molecular Weight: 304.528
• Mol file: 959399-22-5.mol

Synonyms:C₁₇H₂₄OSSi

Chemical Property of C₁₇H₂₄OSSi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₇H₂₄OSSi

There total 1 articles about C₁₇H₂₄OSSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

benzaldehyde (100-52-7) + 3-bromo-2-t-butyldimethylsilyl-thiophene (211737-49-4) → C17H24OSSi (959399-22-5)

Guidance literature:

3-bromo-2-t-butyldimethylsilyl-thiophene; With tert.-butyl lithium; In diethyl ether; hexane; at -78 ℃; for 0.5h;

benzaldehyde; In diethyl ether; hexane; at -78 - -20 ℃; for 1h; Further stages.;

DOI:10.1021/ol702149c

Reference yield: 98.0%

C17H24OSSi (959399-22-5) → 3-<1-(tert-butyldimethylsiloxy)-1-phenylmethyl>thiophene (155791-18-7)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tert.-butyl lithium; In tetrahydrofuran; hexane; at -40 - 0 ℃;

DOI:10.1021/ol702149c

Reference yield: 56.0%

C17H24OSSi (959399-22-5) + propionaldehyde (123-38-6) → C20H30O2SSi

Guidance literature:

C₁₇H₂₄OSSi; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; tert.-butyl lithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.0833333h;

propionaldehyde; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 3h; Further stages.;

DOI:10.1021/ol702149c

upstream raw materials:

benzaldehyde

3-bromo-2-t-butyldimethylsilyl-thiophene

Downstream raw materials:

3-<1-(tert-butyldimethylsiloxy)-1-phenylmethyl>thiophene