6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Base Information

Chemical Name:6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose
CAS No.:1277151-55-9
Molecular Formula:C₁₉H₂₇O₉P*H₃N
Molecular Weight:447.422
Hs Code.:

Synonyms:6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Suppliers and Price of 6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

There total 5 articles about 6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1277151-54-8
6-(benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 1277151-55-9
6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: With ammonium formate; zinc; In tetrahydrofuran; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol2003435

Reference yield:

: 1277151-49-1
benzyl 2-bromo-3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl diisopropylphosphoramidite

: 1277151-55-9
6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / dichloromethane; acetonitrile / 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / nonane; dichloromethane; acetonitrile / 4 h / Inert atmosphere

3: ammonium formate; zinc / tetrahydrofuran; acetonitrile / 2 h / 20 °C / Inert atmosphere

With 1H-tetrazole; tert.-butylhydroperoxide; ammonium formate; zinc; In tetrahydrofuran; nonane; dichloromethane; acetonitrile;
DOI:10.1021/ol2003435

Reference yield:

: C₂₉H₂₉BrF₁₇O₈P

: 1277151-55-9
6-(benzyl ammonium phosphate)-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylhydroperoxide / nonane; dichloromethane; acetonitrile / 4 h / Inert atmosphere

2: ammonium formate; zinc / tetrahydrofuran; acetonitrile / 2 h / 20 °C / Inert atmosphere

With tert.-butylhydroperoxide; ammonium formate; zinc; In tetrahydrofuran; nonane; dichloromethane; acetonitrile;
DOI:10.1021/ol2003435