2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

Base Information

Chemical Name:2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid
CAS No.:1278587-14-6
Molecular Formula:C₃₀H₄₈N₂O₁₀
Molecular Weight:596.719
Hs Code.:

Synonyms:2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

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Chemical Property of 2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

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Technology Process of 2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

There total 10 articles about 2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1278587-13-5
di-tert-butyl 2,2'-(2-(2-(2-((2-tert-butoxy-2-oxoethyl)(2-methoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethylazanediyl)diacetate

: 1278587-14-6
2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201001548

Reference yield:

: 1278587-09-9
benzyl 2-(2-(2-aminoethoxy)phenoxy)ethylcarbamate

: 1278587-14-6
2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: benzene / 20 °C / Molecular sieve; Inert atmosphere

2: sodium tetrahydroborate / methanol / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C / 2585.81 Torr / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere

6: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; palladium 10% on activated carbon; water; hydrogen; potassium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/chem.201001548

Reference yield:

: 1278587-11-3
methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

: 1278587-14-6
2-((2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)(2-tert-butoxy-2-oxoethyl)amino)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 18 h / 20 °C / 2585.81 Torr / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere

3: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; water; hydrogen; potassium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201001548