methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

Base Information

Chemical Name:methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate
CAS No.:1278587-11-3
Molecular Formula:C₂₈H₃₂N₂O₆
Molecular Weight:492.572
Hs Code.:

Synonyms:methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

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Chemical Property of methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

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Technology Process of methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

There total 6 articles about methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1278587-10-2
benzyl 2-(2-(2-(benzylamino)ethoxy)phenoxy)ethylcarbamate

: 96-32-2
bromoacetic acid methyl ester

: 1278587-11-3
methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 8h; Inert atmosphere;
DOI:10.1002/chem.201001548

Reference yield:

: 1278587-09-9
benzyl 2-(2-(2-aminoethoxy)phenoxy)ethylcarbamate

: 1278587-11-3
methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 20 °C / Molecular sieve; Inert atmosphere

2: sodium tetrahydroborate / methanol / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1002/chem.201001548

Reference yield:

: 1278587-08-8
benzyl (2-(2-(2-tert-butoxycarbonylamino)ethoxy)phenoxy)ethylcarbamate

: 1278587-11-3
methyl 2-(benzyl(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)amino)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: benzene / 20 °C / Molecular sieve; Inert atmosphere

3: sodium tetrahydroborate / methanol / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere

With sodium tetrahydroborate; potassium carbonate; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1002/chem.201001548