2,4-dimethoxyphenyl benzoate

Base Information

• Chemical Name: 2,4-dimethoxyphenyl benzoate
• CAS No.: 18093-01-1
• Molecular Formula: C₁₅H₁₄O₄
• Molecular Weight: 258.274
• Mol file: 18093-01-1.mol

Synonyms:2,4-dimethoxyphenyl benzoate

Chemical Property of 2,4-dimethoxyphenyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dimethoxyphenyl benzoate

There total 9 articles about 2,4-dimethoxyphenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

2,4-dimethoxyphenol (13330-65-9) + benzoic acid (65-85-0,8013-63-6) → 2,4-dimethoxyphenyl benzoate (18093-01-1)

Guidance literature:

With potassium hypophosphite; iodine; sodium sulfate; In neat (no solvent); at 20 ℃; for 0.333333h; Reagent/catalyst; Milling; Green chemistry;

DOI:10.1039/d0ra09437d

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-Benzoyloxy-5-methoxy-phenol (88874-66-2) → 2,4-dimethoxyphenyl benzoate (18093-01-1)

Guidance literature:

With diethyl ether; at -10 ℃;

DOI:10.1039/jr9490003189

Reference yield:

dibenzoyl peroxide (94-36-0) → 2,4-dimethoxyphenyl benzoate (18093-01-1)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform

2: diethyl ether / -10 °C

With diethyl ether; chloroform;

DOI:10.1039/jr9490003189

upstream raw materials:

diazomethane

2-Benzoyloxy-5-methoxy-phenol

4-benzoyloxy-resorcinol

methyl iodide

Downstream raw materials:

benzoic acid