(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

Base Information

Chemical Name:(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide
CAS No.:1415249-82-9
Molecular Formula:C₁₉H₁₇FN₆OS
Molecular Weight:396.448
Hs Code.:

Synonyms:(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

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Chemical Property of (rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

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Technology Process of (rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

There total 1 articles about (rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 420-04-2
CYANAMID

: 1415249-81-8
4-(4-fluoro-2-methoxyphenyl)-N-{3-[(methylsulfanyl)methyl]phenyl}-1,3,5-triazin-2-amine

: 1415249-82-9
(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

Guidance literature:: With N-bromophthalimide; potassium tert-butylate; In methanol; at 20 ℃; for 2h;

Reference yield:

: 1415249-82-9
(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

: 1415249-00-1,1415249-03-4,1415249-07-8
(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)oxido-λ6-sulfanylidene]cyanamide

Guidance literature:: With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; at 0 - 20 ℃; for 22h;

Reference yield:

: 1415249-82-9
(rac)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)-λ6-sulfanylidene]cyanamide

: (S)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)oxido-λ6-sulfanylidene]cyanamide

: (R)-[(3-{[4-(4-fluoro-2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}benzyl)(methyl)oxido-λ6-sulfanylidene]cyanamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; 3-chloro-benzenecarboperoxoic acid / ethanol / 22 h / 0 - 20 °C

2: chiralpak IA column / ethanol / 20 °C / Resolution of racemate

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol;