ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

Base Information

Chemical Name:ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate
CAS No.:953054-20-1
Molecular Formula:C₂₀H₂₃NO₅S
Molecular Weight:389.472
Hs Code.:

Synonyms:ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

Chemical Property:

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Technology Process of ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

There total 1 articles about ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 37746-78-4
4-bromo-trans-crotonic acid ethyl ester

: 90312-02-0
N-(2-hydroxymethylphenyl)-4-methylbenzenesulfonamide

: 953054-20-1
ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃;
DOI:10.1016/j.tet.2007.07.007

Reference yield:

: 953054-20-1
ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

: 953054-27-8
(E)-ethyl 4-(N-(2-formylphenyl)-4-methylphenylsulfonamido)but-2-enoate

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2007.07.007

Reference yield:

: 953054-20-1
ethyl-(2E)-4-[[2-(hydroxymethyl)phenyl][(4-methylphenyl)sulfonyl]amino]-2-butenoate

: cis-3-d-1,3,3a,4,5,9b-hexahydro-5-[(4-methylphenyl)sulfonyl]-2H-furo[3,2-c]quinolin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: MnO₂ / CH₂Cl₂ / 2 h / 20 °C

2: 35 mg / Bu₃SnD; AIBN / benzene / 3 h / Heating

With manganese(IV) oxide; 2,2'-azobis(isobutyronitrile); tributyltin deuteride; In dichloromethane; benzene;
DOI:10.1016/j.tet.2007.07.007