2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile

Base Information

• Chemical Name: 2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile
• CAS No.: 143210-01-9
• Molecular Formula: C13H10 Cl F3 N2
• Molecular Weight: 286.684

Synonyms:2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile

Chemical Property of 2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile

Chemical Property:

• PSA: 27.03000
• LogP: 3.77898

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile

There total 1 articles about 2-(4-chlorop henyl)-4，5-dihydro-1-methyl-5-(trifluoromethyl)-1H-pyr role-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(p-chlorophenyl)-N-(trifluoromethyl)sarcosine + acrylonitrile (107-13-1,25014-41-9) → 2-(p-chlorophenyl)-1-methyl-5-(trifluoromethyl)-2-pyrroline-3-carbonitrile (143210-01-9)

Guidance literature:

With acetic anhydride; triethylamine; In ethyl acetate; acetonitrile;

Reference yield: 72.7%

2-(p-chlorophenyl)-1-methyl-5-(trifluoromethyl)-2-pyrroline-3-carbonitrile (143210-01-9) → 2-(p-Chlorophenyl)-1-methyl-5-(trifluoromethyl)-pyrrole-3-carbonitrile (142921-23-1)

Guidance literature:

With bromine; calcium chloride; In tetrachloromethane; for 2h; Reflux;

Reference yield:

2-(p-chlorophenyl)-1-methyl-5-(trifluoromethyl)-2-pyrroline-3-carbonitrile (143210-01-9) → 4-chloro-1-(chloromethyl)-2-(p-chlorophenyl)-5-(trifluoromethyl)pyrrole-3-carbonitrile

Guidance literature:

With chlorine; In n-heptane; 1,2-dichloro-benzene;

upstream raw materials:

acrylonitrile

Downstream raw materials:

2-(p-Chlorophenyl)-1-methyl-5-(trifluoromethyl)-pyrrole-3-carbonitrile

4-bromo-2-p-chlorophenyl-1-methyl-5-trifluoromethylpyrrole-3-carbonitrile

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