4-Nitro-1-phenylhexan

Base Information

• Chemical Name: 4-Nitro-1-phenylhexan
• CAS No.: 72760-79-3
• Molecular Formula: C₁₂H₁₇NO₂
• Molecular Weight: 207.272

Synonyms:4-Nitro-1-phenylhexan

Chemical Property of 4-Nitro-1-phenylhexan

Chemical Property:

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Technology Process of 4-Nitro-1-phenylhexan

There total 3 articles about 4-Nitro-1-phenylhexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-iodo-3-phenylpropan (4119-41-9) + 1-Nitropropane (108-03-2) → 4-Nitro-1-phenylhexan (72760-79-3)

Guidance literature:

With (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr₂; potassium tert-butylate; diethylzinc; In 1,4-dioxane; tert-butyl methyl ether; at 40 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Sealed tube; Glovebox;

DOI:10.1021/jacs.7b04312

Reference yield:

3-Phenyl-1-propanol (122-97-4) → 4-Nitro-1-phenylhexan (72760-79-3)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine; triphenylphosphine; 1H-imidazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

2: (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr₂; diethylzinc; potassium tert-butylate / tert-butyl methyl ether; 1,4-dioxane / 24 h / 40 °C / Inert atmosphere; Sealed tube; Glovebox

With 1H-imidazole; (2,9-dimethyl-4,7-diphenyl-1,10-phenantroline)NiBr₂; potassium tert-butylate; iodine; diethylzinc; triphenylphosphine; In 1,4-dioxane; dichloromethane; tert-butyl methyl ether;

DOI:10.1021/jacs.7b04312

Reference yield:

1-Bromo-3-phenylpropane (637-59-2) + 1-Nitropropane (108-03-2) → 4-Nitro-1-phenylhexan (72760-79-3)

Guidance literature:

Multistep reaction; (i) nBuLi, HMPT, THF (ii) /BRN= 2205527/;

DOI:10.1002/hlca.19790620721

upstream raw materials:

1-Bromo-3-phenylpropane

1-Nitropropane

1-iodo-3-phenylpropan

3-Phenyl-1-propanol

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