2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

Base Information

Chemical Name:2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane
CAS No.:107271-60-3
Molecular Formula:C₄₂H₇₀O₂Si₂
Molecular Weight:663.188
Hs Code.:

Synonyms:2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

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Chemical Property of 2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

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Technology Process of 2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

There total 1 articles about 2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-77-4
chloro-trimethyl-silane

: 107271-45-4
1,3-bis(3,5-di-tert-butyl-4-oxocyclohexa-1,5-dienylidene)-2,2,4,4-tetramethylcyclobutane

: 107271-60-3
2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

Guidance literature:: With sodium; In tetrahydrofuran; for 7h; Irradiation;
DOI:10.1021/jo00387a007

Reference yield: 54.0%

: 107271-60-3
2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

: 107271-45-4
1,3-bis(3,5-di-tert-butyl-4-oxocyclohexa-1,5-dienylidene)-2,2,4,4-tetramethylcyclobutane

Guidance literature:: With trimethyl(benzyl)ammonium fluoride; In tetrahydrofuran; for 10h;
DOI:10.1021/jo00387a007

Reference yield:

: 107271-60-3
2,2,4,4,-tetramethyl-1,3-bis<3,5-di-tert-butyl-4-(trimethylsiloxy)phenyl>bicyclo<1.1.0>butane

: 107271-59-0
disodium salt of 2,2,4,4,-tetramethyl-1,3-bis(3,5-di-tert-butyl-4-hydroxyphenyl)bicyclo<1.1.0>butane

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / benzyltrimethylammonium fluoride / tetrahydrofuran / 10 h

2: 55 percent / Na / tetrahydrofuran / 15 h / Heating

With sodium; trimethyl(benzyl)ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/jo00387a007