[4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol

Base Information

• Chemical Name: [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol
• CAS No.: 1160928-60-8
• Molecular Formula: C₂₅H₃₄N₂O₉
• Molecular Weight: 506.553

Synonyms:[4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol

Chemical Property of [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol

Chemical Property:

Purity/Quality:

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Technology Process of [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol

There total 2 articles about [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

13-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,4,7,10-tetraoxa-13-azacyclopentadecane (1160928-61-9) + 6-nitroveratraldehyde (20357-25-9) → [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol (1160928-60-8)

Guidance literature:

13-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,4,7,10-tetraoxa-13-azacyclopentadecane; 6-nitroveratraldehyde; With tri-1-napthylphosphine; potassium carbonate; palladium dichloride; In tetrahydrofuran; at 23 - 60 ℃; for 24.5h;

With water; In tetrahydrofuran; diethyl ether;

DOI:10.1021/ol900902z

Reference yield: 12.0%

[4-(1-aza-15-crown-5)phenyl]-(4,5-dimethoxy-2-nitrophenyl)-methanone (1160928-59-5) → [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol (1160928-60-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.5h;

DOI:10.1021/ol900902z

Reference yield: 57.0%

[4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrophenyl)methanol (1160928-60-8) → [4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrosophenyl)methanone (1160928-62-0)

Guidance literature:

In acetonitrile; at 25 ℃; for 4h; Quantum yield; Photolysis;

DOI:10.1021/ol900902z

upstream raw materials:

13-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,4,7,10-tetraoxa-13-azacyclopentadecane

6-nitroveratraldehyde

[4-(1-aza-15-crown-5)phenyl]-(4,5-dimethoxy-2-nitrophenyl)-methanone

Downstream raw materials:

[4-(1,4,7,10-tetraoxa-13-azacyclopentadec-13-yl)phenyl](4,5-dimethoxy-2-nitrosophenyl)methanone

Hg((C₂H₄O)4C₂H₄NC₆H₄CH(OH)C₆H₂(NO₂)(OCH₃)2)(ClO₄)⁽¹⁺⁾*ClO₄^(1-)=Hg((C₂H₄O)4C₂H₄NC₆H₄CH(OH)C₆H₂(NO₂)(OCH₃)2)(ClO₄)2

C₂₅H₃₄N₂NaO₉⁽¹⁺⁾*ClO₄^(1-)

C₂₅H₃₄KN₂O₉⁽¹⁺⁾*ClO₄^(1-)

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