N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

Base Information

Chemical Name:N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide
CAS No.:904927-44-2
Molecular Formula:C₂₆H₃₀N₂O₆
Molecular Weight:466.534
Hs Code.:

Synonyms:N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

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Chemical Property of N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

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Technology Process of N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

There total 2 articles about N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 56598-30-2
(S)-N-1-ethoxycarbonyl-2-phenylethylacrylamide

: 904927-44-2
N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

Guidance literature:: PhCH=RuCH[(Mes)NCH=CHN(Mes)](PCy₃)Cl₂; In dichloromethane; at 40 ℃; for 4h;
DOI:10.1002/chem.200501123

Reference yield:

: 3182-93-2
(L)-phenylalanine ethyl ester hydrochloride

: 904927-44-2
N,N'-bis[(S)-1-(ethoxycarbonyl)-2-phenylethyl]fumaric diamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 4 h / 20 °C

2: 97 percent / PhCH=RuCH[(Mes)NCH=CHN(Mes)](PCy₃)Cl₂ / CH₂Cl₂ / 4 h / 40 °C

With triethylamine; PhCH=RuCH[(Mes)NCH=CHN(Mes)](PCy₃)Cl₂; In dichloromethane;
DOI:10.1002/chem.200501123