(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

Base Information

Chemical Name:(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid
CAS No.:1086703-05-0
Molecular Formula:C₁₄H₁₈INO₅
Molecular Weight:407.205
Hs Code.:

Synonyms:(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

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Chemical Property of (S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

Chemical Property:

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Technology Process of (S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

There total 2 articles about (S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1086703-03-8
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

: 1086703-05-0
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

Guidance literature:: (S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid; With triethylsilane; trifluoroacetic acid; at 20 ℃;

With sodium hydroxide; di-tert-butyl dicarbonate; In 1,4-dioxane; water; at 20 ℃;
DOI:10.1055/s-2008-1078209

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₉H₁₀INO₃

: 1086703-05-0
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

Guidance literature:: di-tert-butyl dicarbonate; C₉H₁₀INO₃; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 4h;

With hydrogenchloride; In water; pH=2 - 3;
DOI:10.1002/chem.201000924

Reference yield:

: 1086703-05-0
(S)-2-(tert-butoxycarbonyl(methyl)amino)-2-(4-hydroxy-3-iodophenyl)acetic acid

: 5959-29-5
S-(+)-2-amino-n-butyric acid hydrochloride

: C₁₈H₂₅IN₂O₆

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;