methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

Base Information

Chemical Name:methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate
CAS No.:1373822-47-9
Molecular Formula:C₂₈H₂₃ClN₄O₄S
Molecular Weight:547.034
Hs Code.:

Synonyms:methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

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Chemical Property of methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

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Technology Process of methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

There total 4 articles about methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: C₂₈H₂₅ClN₄O₅S

: 124-41-4
sodium methylate

: 1373822-47-9
methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

Guidance literature:: With methanol; at 90 ℃; for 1h;
DOI:10.1021/jm300037x

Reference yield:

: 43018-72-0
p-chlorophenoxyacetaldehyde

: 1373822-47-9
methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 1 h / 20 °C

2: sodium tris(acetoxy)borohydride / 20 °C

3: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 23 °C

4: methanol / 1 h / 90 °C

With methanol; dmap; sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm300037x

Reference yield:

: 7377-26-6
4-Methoxycarbonylbenzoyl chloride

: 1373822-47-9
methyl 4-(2-(benzylthio)-7-(2-(4-chlorophenoxy)ethyl)-6-oxo-6,7-dihydro-1H-purin-8-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 23 °C

2: methanol / 1 h / 90 °C

With methanol; dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jm300037x