Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

Base Information

Chemical Name:Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4
CAS No.:87306-32-9
Molecular Formula:C₂₄H₂₀B*C₄₃H₄₂CoNP₃S
Molecular Weight:1076.03
Hs Code.:

Co(C<sub>6</sub>H<sub>12</sub>N(P(C<sub>6</sub>H<sub>5</sub>)2)3)(CS)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=Co(C<sub>6</sub>H<sub>12</sub>N(P(C<sub>6</sub>H<sub>5</sub>)2)3)CSB(C<sub>6</sub>H<sub>5</sub>)4

Synonyms:Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

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Chemical Property of Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

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Technology Process of Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

There total 4 articles about Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 53687-39-1
(tris[2-(diphenylphsophino)ethyl]amino)CoH

: 143-66-8
sodium tetraphenyl borate

: 87306-32-9
Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

: 87306-30-7
(tris[2-(diphenylphsophino)ethyl]amino)Co(η2-CS2)

Guidance literature:: With carbon disulfide; In tetrahydrofuran; CS2 vapors were bubled through a suspn. of complex for 5 min, N2 atm.; pptn. with ethanol, washing with ethanol and petroleum ether; elem. anal.;

Reference yield: 45.0%

: 88383-71-5,87306-35-2
C₄₉H₄₇CoN₂P₃S

: 143-66-8
sodium tetraphenyl borate

: 333-27-7
methyl trifluoromethanesulfonate

: 87306-32-9
[(N(CH₂CH₂P(C₆H₅)2)3)Co(CS)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[(N(C₂H₄P(C₆H₅)2)3)Co(CS)]B(C₆H₅)4

Guidance literature:: In dichloromethane; addn. of CH3OSO2CF3 to Co complex soln. under N2; after 1h addn. of NaBPh4 in n-butanol; partial evapn.; crystn.; elem. anal.;
DOI:10.1016/0022-328X(84)80509-4

Reference yield: 30.0%

: 87306-34-1
Co(C₆H₁₂N(P(C₆H₅)2)3)(CS₂CH₃)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CS₂CH₃B(C₆H₅)4

: 87306-32-9
Co(C₆H₁₂N(P(C₆H₅)2)3)(CS)⁽¹⁺⁾*B(C₆H₅)4^(1-)=Co(C₆H₁₂N(P(C₆H₅)2)3)CSB(C₆H₅)4

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; a hot suspn. of complex in THF was treated with large excess of NaBH4 in ethanol with stirring and left standing overnight, N2 atm.; washing with ethanol and petroleum ether; elem. anal.;