2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1352336-46-9
Molecular Formula:C₁₅H₂₃BO₅
Molecular Weight:294.156
Hs Code.:

Synonyms:2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 3 articles about 2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37942-01-1
5-bromo-2-methoxyphenol

: 1352336-46-9
2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 9 h / Inert atmosphere; Reflux

2.1: tert.-butyl lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C

2.3: pH 3

3.1: dichloromethane / 26 h / 20 °C

With tert.-butyl lithium; potassium carbonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmc.2011.10.030

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1225441-53-1
4-methoxy-3-(methoxymethoxy)phenylboronic acid

: 1352336-46-9
2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: In dichloromethane; at 20 ℃; for 26h;
DOI:10.1016/j.bmc.2011.10.030

Reference yield:

: 623550-16-3
4-bromo-1-methoxy-2-(methoxymethoxy)benzene

: 1352336-46-9
2-[4-methoxy-3-(methoxymethoxy)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C

1.3: pH 3

2.1: dichloromethane / 26 h / 20 °C

With tert.-butyl lithium; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2011.10.030