C₃₃H₂₇BN₂O₂

Base Information

Chemical Name:C₃₃H₂₇BN₂O₂
CAS No.:1357066-47-7
Molecular Formula:C₃₃H₂₇BN₂O₂
Molecular Weight:494.401
Hs Code.:

C<sub>33</sub>H<sub>27</sub>BN<sub>2</sub>O<sub>2</sub>

Synonyms:C₃₃H₂₇BN₂O₂

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Chemical Property of C₃₃H₂₇BN₂O₂

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Technology Process of C₃₃H₂₇BN₂O₂

There total 9 articles about C₃₃H₂₇BN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 121-43-7,63156-11-6
Trimethyl borate

: C₃₃H₂₅BrN₂

: 1357066-47-7
C₃₃H₂₇BN₂O₂

Guidance literature:: C₃₃H₂₅BrN₂; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

Trimethyl borate; In tetrahydrofuran; at -78 ℃; for 25h;

With hydrogenchloride; water; In tetrahydrofuran; at 0 ℃; for 0.166667h;

Reference yield:

: 6267-02-3
9,9‐dimethyl‐10H‐acridine

: 1357066-47-7
C₃₃H₂₇BN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 120 °C

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 6 h / 0 °C

3.1: caesium carbonate; tri-tert-butyl phosphine / palladium diacetate / toluene / 4 h / 120 °C

4.1: caesium carbonate; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt / palladium diacetate / ISOPROPYLAMIDE / 4 h / 190 °C

5.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 24 h / 180 °C

6.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

6.2: 25 h / -78 °C

6.3: 0.17 h / 0 °C

With N-Bromosuccinimide; n-butyllithium; 18-crown-6 ether; tri-tert-butyl phosphine; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; copper; potassium carbonate; caesium carbonate; sodium t-butanolate; palladium diacetate; In tetrahydrofuran; ISOPROPYLAMIDE; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene;

Reference yield:

: 73183-55-8
α,α-Dimethyl-2-(phenylamino)benzolmethanol

: 1357066-47-7
C₃₃H₂₇BN₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: phosphoric acid / 12 h / 20 °C

2.1: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 12 h / 120 °C

3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 6 h / 0 °C

4.1: caesium carbonate; tri-tert-butyl phosphine / palladium diacetate / toluene / 4 h / 120 °C

5.1: caesium carbonate; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt / palladium diacetate / ISOPROPYLAMIDE / 4 h / 190 °C

6.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 24 h / 180 °C

7.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

7.2: 25 h / -78 °C

7.3: 0.17 h / 0 °C

With N-Bromosuccinimide; n-butyllithium; 18-crown-6 ether; tri-tert-butyl phosphine; di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; phosphoric acid; copper; potassium carbonate; caesium carbonate; sodium t-butanolate; palladium diacetate; In tetrahydrofuran; ISOPROPYLAMIDE; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene;