9,9-Dimethyl-9,10-dihydroacridine

Base Information

• Chemical Name: 9,9-Dimethyl-9,10-dihydroacridine
• CAS No.: 6267-02-3
• Deprecated CAS: 1643983-90-7,2295813-02-2,2304441-41-4,475150-56-2
• Molecular Formula: C15H15N
• Molecular Weight: 209.291
• Hs Code.: 29339900
• European Community (EC) Number: 228-436-9
• NSC Number: 36671
• UNII: TOD9JH3PHC
• DSSTox Substance ID: DTXSID4064185
• Nikkaji Number: J29.111K
• Wikidata: Q72464880
• Mol file: 6267-02-3.mol

Synonyms:9,9-dimethylcarbazine

Chemical Property of 9,9-Dimethyl-9,10-dihydroacridine

Chemical Property:

• Vapor Pressure: 0.000147mmHg at 25°C
• Melting Point: 120-126℃
• Refractive Index: 1.577
• Boiling Point: 332.3 °C at 760 mmHg
• PKA: 2.05±0.40(Predicted)
• Flash Point: 162.3 °C
• PSA: 12.03000
• Density: 1.043 g/cm³
• LogP: 4.20750
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 209.120449483
• Heavy Atom Count: 16
• Complexity: 234

Purity/Quality:

98% ^*data from raw suppliers

9,9-Dimethyl-9,10-dihydroacridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C2=CC=CC=C2NC3=CC=CC=C31)C

Technology Process of 9,9-Dimethyl-9,10-dihydroacridine

There total 21 articles about 9,9-Dimethyl-9,10-dihydroacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.7%

α,α-Dimethyl-2-(phenylamino)benzolmethanol (73183-55-8) → 9,9‐dimethyl‐10H‐acridine (6267-02-3)

Guidance literature:

With phosphoric acid; In water; at 35 ℃; for 2h;

Reference yield: 90.0%

N-(2-isopropylphenyl)aniline (38158-59-7) → 9,9‐dimethyl‐10H‐acridine (6267-02-3)

Guidance literature:

With sulfuric acid; at 20 ℃; for 5h;

Reference yield: 81.0%

Methyl N-phenylanthranilate (35708-19-1) + methylmagnesium bromide (75-16-1) → 9,9‐dimethyl‐10H‐acridine (6267-02-3)

Guidance literature:

In tetrahydrofuran; at 0 ℃;

upstream raw materials:

methyl magnesium iodide

9-methyl-acridine

diphenylamine

acetone

Downstream raw materials:

N-benzyl-9,9-dimethyl-9,10-dihydroacridine

9-methyl-acridine

2-bromo-9,9-dimethyl-10-phenyl-9,10-dihydro-acridine

N-(2-chlorophenyl)-9,9-dimethyl-10-phenyl-9,10-dihydroacridin-2-amine

Refernces

• 1、 -. "Carbazole derivatives and organoelectro luminescent device using the same". Paragraph 0366; 0379-0384. . Retrieved 2020/11/28.
• 2、 -. "Photoelectric conversion element, imaging device, optical sensor, and method of using photoelectric conversion element". Page/Page column 96-98. . Retrieved 2020/02/29.