[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Base Information

Chemical Name:[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol
CAS No.:201213-67-4
Molecular Formula:C₂₃H₃₈Cl₂O₉
Molecular Weight:529.455
Hs Code.:

Synonyms:[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

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Chemical Property of [3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

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Technology Process of [3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

There total 4 articles about [3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 201213-63-0
methyl 3,5-bis(12-chloro-1,4,7,10-tetraoxadodecyl)benzoate

: 201213-67-4
[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 15h; Ambient temperature;
DOI:10.1139/v97-165

Reference yield:

: 638-56-2,27252-69-3
1,11-dichloro-3,6,9-trioxaundecane

: 201213-67-4
[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 110 deg C, 3 h, 2.) DMF, 50 deg C, 5 d

2: 94 percent / LAH / tetrahydrofuran / 15 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran;
DOI:10.1139/v97-165

Reference yield:

: 112-60-7
Tetraethylene glycol

: 201213-67-4
[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂, pyridine / toluene / 36 h / Heating

2: 1.) NaH / 1.) DMF, 110 deg C, 3 h, 2.) DMF, 50 deg C, 5 d

3: 94 percent / LAH / tetrahydrofuran / 15 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; thionyl chloride; sodium hydride; In tetrahydrofuran; toluene;
DOI:10.1139/v97-165