3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

Base Information

Chemical Name:3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde
CAS No.:201213-69-6
Molecular Formula:C₂₃H₃₆Cl₂O₉
Molecular Weight:527.439
Hs Code.:

Synonyms:3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

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Chemical Property of 3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

Chemical Property:

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Technology Process of 3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

There total 5 articles about 3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 201213-67-4
[3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phenyl]-methanol

: 201213-69-6
3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1139/v97-165

Reference yield:

: 638-56-2,27252-69-3
1,11-dichloro-3,6,9-trioxaundecane

: 201213-69-6
3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 110 deg C, 3 h, 2.) DMF, 50 deg C, 5 d

2: 94 percent / LAH / tetrahydrofuran / 15 h / Ambient temperature

3: 86 percent / PCC / CH₂Cl₂ / 15 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1139/v97-165

Reference yield:

: 112-60-7
Tetraethylene glycol

: 201213-69-6
3,5-Bis-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, pyridine / toluene / 36 h / Heating

2: 1.) NaH / 1.) DMF, 110 deg C, 3 h, 2.) DMF, 50 deg C, 5 d

3: 94 percent / LAH / tetrahydrofuran / 15 h / Ambient temperature

4: 86 percent / PCC / CH₂Cl₂ / 15 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; thionyl chloride; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1139/v97-165