Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid
CAS No.:141019-69-4
Molecular Formula:C₃₀H₂₈F₃NO₁₀S
Molecular Weight:651.614
Hs Code.:

Synonyms:Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

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Chemical Property of Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

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Technology Process of Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

There total 4 articles about Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 82827-77-8
Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid

: 141019-69-4
Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

Guidance literature:: With pyridine; In dichloromethane; at -20 ℃; for 2h;

Reference yield:

: 13343-62-9,347411-88-5
benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 141019-69-4
Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Pyridin / a) -45 deg C, 2 h, b) RT, 8 h

2: Pyridin / CH₂Cl₂ / -30 °C

With pyridine; In dichloromethane;
DOI:10.1016/0008-6215(93)84151-U

Reference yield:

: 98-88-4
benzoyl chloride

: 141019-69-4
Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Pyridin / a) -45 deg C, 2 h, b) RT, 8 h

2: Pyridin / CH₂Cl₂ / -30 °C

With pyridine; In dichloromethane;
DOI:10.1016/0008-6215(93)84151-U