N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

Base Information

Chemical Name:N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide
CAS No.:1425927-10-1
Molecular Formula:C₁₈H₁₈N₂O₄S
Molecular Weight:358.418
Hs Code.:

Synonyms:N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

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Chemical Property of N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

Chemical Property:

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Technology Process of N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

There total 6 articles about N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 10130-87-7
o-Methoxybenzenesulfonyl chloride

: 1425927-75-8
6-amino-1,3-dimethyl-6-quinolin-2-(1H)-one

: 1425927-10-1
N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

Guidance literature:: With pyridine;
DOI:10.1021/acs.jmedchem.6b01583

Reference yield:

: 2721-59-7
3-methylcarbostyril

: 1425927-10-1
N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; nitric acid / 2 h / Cooling with ice

2: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Cooling with ice

3: iron; ammonium chloride; water / tetrahydrofuran; ethanol / 3 h / 50 °C

4: triethylamine / dichloromethane / 16 h / 0 - 20 °C

With sulfuric acid; potassium tert-butylate; water; nitric acid; iron; ammonium chloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 1425927-74-7
1,3-dimethyl-6-nitroquinolin-2-(1H)-one

: 1425927-10-1
N-(1,3-dimethyl-2-oxo-1,2-dihydroquinolin-6-yl)-2-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: iron; ammonium chloride; water / tetrahydrofuran; ethanol / 3 h / 50 °C

2: triethylamine / dichloromethane / 16 h / 0 - 20 °C

With water; iron; ammonium chloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;