19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Base Information

Chemical Name:19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene
CAS No.:122475-92-7
Molecular Formula:C₂₄H₃₂O₆S
Molecular Weight:448.58
Hs Code.:

Synonyms:19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Suppliers and Price of 19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

There total 5 articles about 19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 122475-96-1
19-methoxy-17-methyl-8-phenylthiomethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

: 122475-92-7
19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: With sodium periodate; In methanol; water; for 24h;

Reference yield:

: 28544-88-9
2,2'-(2-methylenepropane-1,3-diyldioxy)bisethanol

: 122475-92-7
19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / NaH / tetrahydrofuran / 2 h / Heating

2: 74 percent / p-toluenesulfonic acid / 12 h / Ambient temperature

3: 78 percent / sodium metaperiodate / methanol; H₂O / 24 h

With sodium periodate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water;

Reference yield:

: 6327-85-1
2,6-bis(hydroxymethyl)-4-methyl-anisole

: 122475-92-7
19-methoxy-17-methyl-8-phenylsulfinylmethyl-3,6,10,13-tetraoxabicyclo<13.3.1>nonadeca-1(19),15,17-triene

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / PBr₃ / CH₂Cl₂ / 6 h / Ambient temperature

2: 65 percent / NaH / tetrahydrofuran / 2 h / Heating

3: 74 percent / p-toluenesulfonic acid / 12 h / Ambient temperature

4: 78 percent / sodium metaperiodate / methanol; H₂O / 24 h

With sodium periodate; phosphorus tribromide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water;