di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

Base Information

Chemical Name:di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate
CAS No.:1202870-44-7
Molecular Formula:C₃₃H₄₉N₃O₆
Molecular Weight:583.769
Hs Code.:

Synonyms:di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

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Chemical Property of di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

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Technology Process of di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

There total 4 articles about di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 501-53-1,94274-21-2
benzyl chloroformate

: 149525-65-5
1,3,5-triethyl-2,4,6-tris(aminomethyl)benzene

: 1202870-44-7
di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; at 0 - 20 ℃; for 6h;
DOI:10.1021/acs.joc.0c01206

Reference yield:

: 181058-08-2
1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene

: 1202870-44-7
di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / N,N-dimethyl-formamide / 48 h

2: 5%-palladium/activated carbon; hydrogen / methanol / 72 h

3: sodium hydroxide / 1,4-dioxane; water / 6 h / 0 - 20 °C

With sodium azide; 5%-palladium/activated carbon; hydrogen; sodium hydroxide; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.0c01206

Reference yield:

: 190779-62-5
1,3,5-tris(azidomethyl)-2,4,6-triethylbenzene

: 1202870-44-7
di-tert-butyl ((5-((((benzyloxy)carbonyl)amino)methyl)-2,4,6-triethyl-1,3-phenylene)bis(methylene)) dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen / methanol / 72 h

2: sodium hydroxide / 1,4-dioxane; water / 6 h / 0 - 20 °C

With 5%-palladium/activated carbon; hydrogen; sodium hydroxide; In 1,4-dioxane; methanol; water;
DOI:10.1021/acs.joc.0c01206