methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene)

Base Information

• Chemical Name: methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene)
• CAS No.: 1367715-91-0
• Molecular Formula: C₂₂H₂₂O₁₀
• Molecular Weight: 446.411
• Mol file: 1367715-91-0.mol

Synonyms:methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene)

Chemical Property of methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene)

There total 3 articles about methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,4-diacetylphloroglucinol (2161-86-6) + acetaldehyde (75-07-0,9002-91-9) → methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene) (1367715-91-0)

Guidance literature:

With silica sulphuric acid (SSA); In neat (no solvent); at 20 ℃; Sonication;

DOI:10.1039/d0nj06114j

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + acetaldehyde (75-07-0,9002-91-9) → methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene) (1367715-91-0)

Guidance literature:

for 0.25h;

DOI:10.1016/j.bmcl.2012.01.089

Reference yield:

3,5-dihydroxyphenol (108-73-6) → methyl-methylene-bis-(3,5-diacetyl-2,4,6-trihydroxybenzene) (1367715-91-0)

Guidance literature:

Multi-step reaction with 2 steps

1: silica sulphuric acid (SSA) / 60 °C / Sonication

2: silica sulphuric acid (SSA) / neat (no solvent) / 20 °C / Sonication

With silica sulphuric acid (SSA); In neat (no solvent);

DOI:10.1039/d0nj06114j

upstream raw materials:

formaldehyd

acetaldehyde

2,4-diacetylphloroglucinol

3,5-dihydroxyphenol