3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid

Base Information

• Chemical Name: 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid
• CAS No.: 128398-47-0
• Molecular Formula: C₂₀H₂₀N₂O₅
• Molecular Weight: 368.389

Synonyms:3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid

Chemical Property of 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid

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Technology Process of 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid

There total 1 articles about 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3-(benzoyl)amino-7,7-dimetyl-5-oxo-5,6,7,8-tetrahydro-2H-1-benzopyran-2-one (125812-05-7) + sodium glycinate (6000-44-8) → 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid (128398-47-0)

Guidance literature:

In N,N-dimethyl-formamide; Heating;

DOI:10.3987/COM-89-S8

Reference yield: 83.0%

methanol (67-56-1) + 3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid (128398-47-0) → methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetate (128398-48-1)

Guidance literature:

With hydrogenchloride;

DOI:10.3987/COM-89-S8

Reference yield: 80.0%

3-(Benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetic acid (128398-47-0) → 3-(benzoylamino)-2,5,6,7,8-hexahydro-8,8-dimethyl-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetic acid (128398-52-7)

Guidance literature:

With sodium azide; sulfuric acid; In chloroform; 1.) 0 deg C, 1.5 h, 2.) RT, 2 h;

DOI:10.3987/COM-89-S8

upstream raw materials:

3-(benzoyl)amino-7,7-dimetyl-5-oxo-5,6,7,8-tetrahydro-2H-1-benzopyran-2-one

sodium glycinate

Downstream raw materials:

methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-7,7-dimethyl-2,5-dioxo-1(2H)-quinolineacetate

3-(benzoylamino)-2,5,6,7,8-hexahydro-8,8-dimethyl-2,5-dioxo-1H-pyrido<3,2-c>azepine-1-acetic acid

N-(7,7-Dimethyl-2,5-dioxo-1,2,5,6,7,8-hexahydro-quinolin-3-yl)-benzamide

N-<1,2,5,6,7,8-hexahydro-1-(isocyanatomethyl)-7,7-dimethyl-2,5-dioxo-3-quinolinyl>benzamide

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