(4S)-(-)-perillyl butyl ether

Base Information

Chemical Name:(4S)-(-)-perillyl butyl ether
CAS No.:146659-07-6
Molecular Formula:C₁₄H₂₄O
Molecular Weight:208.344
Hs Code.:

Synonyms:(4S)-(-)-perillyl butyl ether

Suppliers and Price of (4S)-(-)-perillyl butyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-(-)-perillyl butyl ether

Chemical Property:

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Technology Process of (4S)-(-)-perillyl butyl ether

There total 6 articles about (4S)-(-)-perillyl butyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-65-9
1-bromo-butane

: 536-59-4,18457-55-1
(-)-perillyl alcohol

: 146659-07-6
(4S)-(-)-perillyl butyl ether

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 10h; Heating;
DOI:10.1016/S0040-4020(01)86265-7

Reference yield:

: 7785-70-8,25766-18-1
(+)-α-pinene

: 146659-07-6
(4S)-(-)-perillyl butyl ether

Guidance literature:: Multi-step reaction with 4 steps

2: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature

3: ammonium nitrate / nitromethane / 4 h / 80 °C

4: 90 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

With ammonium nitrate; dihydrogen peroxide; sodium hydride; potassium hydrogencarbonate; benzonitrile; In tetrahydrofuran; methanol; nitromethane;
DOI:10.1016/S0040-4020(01)86265-7

Reference yield:

: 18172-67-3,19902-08-0,25719-60-2
beta-pinene

: 146659-07-6
(4S)-(-)-perillyl butyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature

2: ammonium nitrate / nitromethane / 4 h / 80 °C

3: 90 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

With ammonium nitrate; dihydrogen peroxide; sodium hydride; potassium hydrogencarbonate; benzonitrile; In tetrahydrofuran; methanol; nitromethane;
DOI:10.1016/S0040-4020(01)86265-7