N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

Base Information

Chemical Name:N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide
CAS No.:13232-98-9
Molecular Formula:C₃₂H₃₂BrNO₅
Molecular Weight:590.514
Hs Code.:

Synonyms:N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

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Technology Process of N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

There total 9 articles about N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 892805-32-2
N-(4'-benzyloxy-3'-methoxyphenylethyl)-2-(2-bromo-5-hydroxy-4-methoxyphenyl)acetamide

: 100-44-7
benzyl chloride

: 13232-98-9
N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

Guidance literature:: With potassium carbonate; In ethanol; for 6h; Heating;
DOI:10.1055/s-2006-926410

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 13232-98-9
N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: AlCl₃ / toluene

1.2: Br₂; AcOH / CH₂Cl₂ / -78 °C

2.1: 75 percent / NH₃; H₂ / Ra-Ni catalyst / ethanol / 70 °C / 7600 Torr

3.1: 61 percent / 3 h / 180 °C

4.1: 80 percent / K₂CO₃ / ethanol / 6 h / Heating

With aluminium trichloride; ammonia; hydrogen; potassium carbonate; Ra-Ni catalyst; In ethanol; toluene;
DOI:10.1055/s-2006-926410

Reference yield:

: 4468-59-1
4-hydroxy-3-methoxyphenylacetonitrile

: 13232-98-9
N-(4'-benzyloxy-2-bromo-4-methoxyphenyl)-N-(4'-benzyloxy-3'-methoxyphenylethyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NH₃; H₂ / Ra-Ni catalyst / ethanol / 70 °C / 7600 Torr

2: 61 percent / 3 h / 180 °C

3: 80 percent / K₂CO₃ / ethanol / 6 h / Heating

With ammonia; hydrogen; potassium carbonate; Ra-Ni catalyst; In ethanol;
DOI:10.1055/s-2006-926410