Technology Process of N,N-dibenzyl-4-(3-methyloxetan-3-yl)aniline
There total 5 articles about N,N-dibenzyl-4-(3-methyloxetan-3-yl)aniline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Wilkinson's catalyst;
In
toluene;
for 1h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / diethyl ether; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: 3.25 h / -78 - 20 °C
1.3: 0.33 h / 20 °C
2.1: potassium hydroxide / chloro(1,5-cyclooctadiene)rhodium(I) dimer / 1,4-dioxane / 6 h / 20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 °C
3.2: kieselguhr
4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
4.2: -78 - 20 °C
5.1: Wilkinson's catalyst / toluene / 1 h / Inert atmosphere; Reflux
With
lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; potassium hydroxide;
Wilkinson's catalyst; chloro(1,5-cyclooctadiene)rhodium(I) dimer;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: Wilkinson's catalyst / toluene / 1 h / Inert atmosphere; Reflux
With
oxalyl dichloride; dimethyl sulfoxide;
Wilkinson's catalyst;
In
dichloromethane; toluene;
![{3-[4-(dibenzylamino)phenyl]oxetan-3-yl}acetaldehyde](/Databaselist/images/loading.webp)
