{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

Base Information

Chemical Name:{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine
CAS No.:1062671-23-1
Molecular Formula:C₂₈H₃₂N₄O₂
Molecular Weight:456.588
Hs Code.:

Synonyms:{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

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Chemical Property of {4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

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Technology Process of {4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

There total 14 articles about {4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 4-benzyloxy-3-ethyl-5-methylbenzoic acid-N'-(2-diethylamino-6-methylpyridine-4-carbonyl)hydrazide

: 1062671-23-1
{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

Guidance literature:: With Burgess Reagent; In tetrahydrofuran; at 110 ℃; for 0.0833333h; Microwave irradiation; Inert atmosphere;
DOI:10.1021/jm4014696

Reference yield:

: 1062671-21-9
4-benzyloxy-3-ethyl-5-methyl-benzoic acid N'-(2-diethylamino-6-methyl-pyridine-4-carbonyl)-hydrazide

: 1062671-23-1
{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

Guidance literature:: With Burgess Reagent; In tetrahydrofuran; at 110 ℃; for 0.0833333h; Microwave irradiation;

Reference yield:

: 1010113-45-7
4-benzyloxy-3-ethyl-5-methylbenzoic acid hydrazide

: 1062671-23-1
{4-[5-(4-benzyloxy-3-ethyl-5-methylphenyl)-[1,3,4]oxadiazol-2-yl]-6-methylpyridin-2-yl}diethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane; N,N-dimethyl-formamide / 1.17 h / 20 °C / Inert atmosphere

2: Burgess Reagent / tetrahydrofuran / 0.08 h / 110 °C / Microwave irradiation; Inert atmosphere

With Burgess Reagent; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm4014696