(2,3-Dimethoxyphenyl)hydrazine

Base Information

Chemical Name:(2,3-Dimethoxyphenyl)hydrazine
CAS No.:53898-99-0
Molecular Formula:C₈H₁₂N₂O₂
Molecular Weight:168.195
Hs Code.:
European Community (EC) Number:802-199-7
Nikkaji Number:J3.146.475G

Synonyms:(2,3-dimethoxyphenyl)hydrazine;SCHEMBL15127718;AKOS006334089;53898-99-0;EN300-1869989

Suppliers and Price of (2,3-Dimethoxyphenyl)hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (2,3-Dimethoxyphenyl)hydrazine

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:168.089877630
Heavy Atom Count:12
Complexity:132

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=CC(=C1OC)NN

Technology Process of (2,3-Dimethoxyphenyl)hydrazine

There total 3 articles about (2,3-Dimethoxyphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 53898-99-0
(2,3-dimethoxyphenyl)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / diphenylphosphoryl azide, triethylamine / tetrahydrofuran / 1.5 h / 60 °C

2: 95 percent / KOH / ethanol / 4 h / Heating

3: 1.) aq. NaNO₂, 6 N aq. HCl, 2.) SnCl₂, concd. HCl, 3.) 10 M aq. NaOH / 1.) 0 deg C, 1.5 h, 2.) 1 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; diphenylphosphoranyl azide; triethylamine; tin(ll) chloride; sodium nitrite; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00084a026

Reference yield:

: 153718-64-0
2,3-dimethoxyphenylcarbamic acid ethyl ester

: 53898-99-0
(2,3-dimethoxyphenyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / KOH / ethanol / 4 h / Heating

2: 1.) aq. NaNO₂, 6 N aq. HCl, 2.) SnCl₂, concd. HCl, 3.) 10 M aq. NaOH / 1.) 0 deg C, 1.5 h, 2.) 1 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; tin(ll) chloride; sodium nitrite; In ethanol;
DOI:10.1021/ja00084a026

Reference yield:

: 6299-67-8
2,3-dimethoxyaniline

: 53898-99-0
(2,3-dimethoxyphenyl)hydrazine

Guidance literature:: With hydrogenchloride; sodium hydroxide; tin(ll) chloride; sodium nitrite; Yield given. Multistep reaction; 1.) 0 deg C, 1.5 h, 2.) 1 h;
DOI:10.1021/ja00084a026