tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane
CAS No.:955930-05-9
Molecular Formula:C₂₀H₃₅BO₃Si
Molecular Weight:362.393
Hs Code.:

Synonyms:tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Suppliers and Price of tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

There total 4 articles about tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1-{[(tert-butyl)(dimethyl)sily]oxy}-3,5-dimethylbenzene

: 73183-34-3
bis(pinacol)diborane

: 955930-05-9
tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Guidance literature:: With C₃₅H₅₂N₂OPtSi₂; at 120 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1246/bcsj.20160391

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 955930-05-9
tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: C₃₅H₅₂N₂OPtSi₂ / 16 h / 120 °C / Sealed tube; Inert atmosphere

With dmap; C₃₅H₅₂N₂OPtSi₂; triethylamine; In dichloromethane;
DOI:10.1246/bcsj.20160391

Reference yield:

: 7463-51-6
4-bromo-3,5-dimethylphenol

: 955930-05-9
tert-butyl(3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole

2: n-butyllithium / -78 °C

With 1H-imidazole; n-butyllithium;
DOI:10.1016/j.ejmech.2017.03.041