(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

Base Information

Chemical Name:(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine
CAS No.:126459-37-8
Molecular Formula:C₂₉H₂₇NO₃
Molecular Weight:437.538
Hs Code.:

Synonyms:(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

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Chemical Property of (4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

Chemical Property:

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Technology Process of (4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

There total 1 articles about (4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126459-30-1
(4S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-oxo-4'-hexynyl)oxazolidine

: 74-88-4
methyl iodide

: 126576-03-2
(4S,1'S,2'R)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

: 126459-37-8
(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jo00298a025

Reference yield: 90.0%

: 126459-37-8
(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

: 126459-40-3
(2S,3S,4S)-2-(N-(9-phenylfluoren-9-yl)amino)-3-hydroxy-4-methyl-6-octynol

Guidance literature:: With potassium hydroxide; In ethanol; for 18h; Heating;
DOI:10.1021/jo00298a025

Reference yield:

: 126459-37-8
(4S,1'S,2'S)-2-oxo-3-(9-phenylfluoren-9-yl)-4-(1'-hydroxy-2'-methyl-4'-hexynyl)oxazolidine

: 126459-48-1
(1S,2S)-2-Methyl-1-[(S)-3-(9-phenyl-9H-fluoren-9-yl)-oxazolidin-4-yl]-hex-4-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / KOH / ethanol / 18 h / Heating

2: 1) TsOH / 2) SiO₂ / 1) THF, 24h

With potassium hydroxide; toluene-4-sulfonic acid; silica gel; In ethanol;
DOI:10.1021/jo00298a025