phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

Base Information

Chemical Name:phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester
CAS No.:1426899-70-8
Molecular Formula:C₂₂H₂₃N₂O₇PS
Molecular Weight:490.474
Hs Code.:

Synonyms:phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

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Chemical Property of phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

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Technology Process of phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

There total 12 articles about phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426899-88-8
phosphoric acid dibenzyl ester 2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]-amino}-ethyl ester

: 1426899-70-8
phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; water;

Reference yield:

: 1426899-85-5
2-(2-o-tolyl-chroman-6-yloxy)-thiazole-5-carboxylic acid lithium salt

: 1426899-70-8
phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 16 h

2.1: 1H-tetrazole / dichloromethane; acetonitrile / 1.17 h / 0 °C

2.2: 0.17 h / 0 °C

3.1: hydrogen; palladium 10% on activated carbon / methanol; water

With 4-methyl-morpholine; 1H-tetrazole; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1426899-86-6
2-(2-o-tolyl-chroman-6-yloxy)-thiazole-5-carboxylic acid (2-hydroxy-ethyl)-amide

: 1426899-70-8
phosphoric acid mono-(2-{[2-((S)-2-o-tolyl-chroman-6-yloxy)-thiazole-5-carbonyl]amino}ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-tetrazole / dichloromethane; acetonitrile / 1.17 h / 0 °C

1.2: 0.17 h / 0 °C

2.1: hydrogen; palladium 10% on activated carbon / methanol; water

With 1H-tetrazole; palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; water; acetonitrile;