C₂₃H₁₆F₃NO₄

Base Information

Chemical Name:C₂₃H₁₆F₃NO₄
CAS No.:1361005-27-7
Molecular Formula:C₂₃H₁₆F₃NO₄
Molecular Weight:427.38
Hs Code.:

C<sub>23</sub>H<sub>16</sub>F<sub>3</sub>NO<sub>4</sub>

Synonyms:C₂₃H₁₆F₃NO₄

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Chemical Property of C₂₃H₁₆F₃NO₄

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Technology Process of C₂₃H₁₆F₃NO₄

There total 6 articles about C₂₃H₁₆F₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1361006-09-8
4-oxo-3-(4-(4-(trifluoromethoxy)phenoxy)phenyl)-1,4-dihydroquinoline-2-carbaldehyde

: 1361005-27-7
C₂₃H₁₆F₃NO₄

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/jm201179h

Reference yield:

: 63478-10-4
2-(2'-anilinyl)-4,4-dimethyl-4,5-dihydro-1,3-oxazole

: 1361005-27-7
C₂₃H₁₆F₃NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / butan-1-ol / 24 h / 130 °C / Inert atmosphere

2.1: caesium carbonate; acetylacetone / 1-methyl-pyrrolidin-2-one / 48 h / 120 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.2: 0.5 h / Inert atmosphere

4.1: selenium(IV) oxide / 1,4-dioxane; water / 5 h / 100 °C / Inert atmosphere

5.1: potassium hydroxide / ethanol; water / 1 h / 20 °C / Inert atmosphere

6.1: sodium tetrahydroborate / methanol / 0.17 h / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; sodium tetrahydroborate; potassium tert-butylate; caesium carbonate; toluene-4-sulfonic acid; acetylacetone; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; ethanol; water; butan-1-ol;
DOI:10.1021/jm201179h

Reference yield:

: 1354745-32-6
2-methyl-3-(4-(4-(trifluoromethoxy)phenoxy)-phenyl)quinolin-4(1H)-one

: 1361005-27-7
C₂₃H₁₆F₃NO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: selenium(IV) oxide / 1,4-dioxane; water / 5 h / 100 °C / Inert atmosphere

3.1: potassium hydroxide / ethanol; water / 1 h / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 0.17 h / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; sodium tetrahydroborate; potassium tert-butylate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water;
DOI:10.1021/jm201179h