tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

Base Information

Chemical Name:tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate
CAS No.:936544-97-7
Molecular Formula:C₂₂H₂₅ClN₄O₂
Molecular Weight:412.919
Hs Code.:

Synonyms:tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

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Chemical Property of tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

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Technology Process of tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

There total 5 articles about tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 936544-96-6
tert-butyl (4-(((2-chloro-3-nitroquinolin-4-yl)amino)methyl)benzyl)carbamate

: 936544-97-7
tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; sodium sulfate; In ethyl acetate; at 20 ℃; for 8h; under 3750.38 Torr; Sealed tube;

Reference yield:

: 70254-44-3
2,4-dihydroxyquinoline

: 936544-97-7
tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid / 70 °C

2: P,P-dichlorophenylphosphine oxide / 135 °C

3: triethylamine

4: hydrogen; palladium 10% on activated carbon; sodium sulfate / ethyl acetate

With P,P-dichlorophenylphosphine oxide; palladium 10% on activated carbon; hydrogen; nitric acid; sodium sulfate; triethylamine; In ethyl acetate;

Reference yield:

: 15151-57-2
2,4-dihydroxy-3-nitroquinoline

: 936544-97-7
tert-butyl (4-(((3-amino-2-chloroquinolin-4-yl)amino)methyl)benzyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: P,P-dichlorophenylphosphine oxide / 135 °C

2: triethylamine

3: hydrogen; palladium 10% on activated carbon; sodium sulfate / ethyl acetate

With P,P-dichlorophenylphosphine oxide; palladium 10% on activated carbon; hydrogen; sodium sulfate; triethylamine; In ethyl acetate;