3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Base Information

Chemical Name:3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose
CAS No.:942622-18-6
Molecular Formula:C₃₉H₆₄O₁₄Si₂
Molecular Weight:813.1
Hs Code.:

Synonyms:3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Suppliers and Price of 3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

There total 4 articles about 3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 942622-17-5
2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

: 98-88-4
benzoyl chloride

: 942622-18-6
3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2007.03.138

Reference yield:

: 942622-16-4
2,1’:4,6-di-O-isopropylidene-4’,6’-O-tetraisopropyldisiloxanilidene sucrose

: 942622-18-6
3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 6 h / 20 °C

2: 97 percent / pyridine / 1 h / 20 °C

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2007.03.138

Reference yield:

: 67909-39-1
2,1′:4,6-di-O-isopropylidene sucrose

: 942622-18-6
3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine; imidazole / dimethylformamide / 8 h / 20 °C

2: 85 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 6 h / 20 °C

3: 97 percent / pyridine / 1 h / 20 °C

With pyridine; 1H-imidazole; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2007.03.138