6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Base Information

Chemical Name:6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose
CAS No.:942622-22-2
Molecular Formula:C₆₃H₉₁NO₂₆Si₂
Molecular Weight:1334.58
Hs Code.:

6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Synonyms:6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

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Chemical Property of 6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

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Technology Process of 6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

There total 13 articles about 6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 942622-21-1
6,1'-di-O-acetyl-3'-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

: 98-88-4
benzoyl chloride

: 942622-22-2
6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: With pyridine; at 20 ℃; for 4h;
DOI:10.1016/j.tetlet.2007.03.138

Reference yield:

: 942622-18-6
3'-O-benzoyl-2,1':4,6-di-O-isopropylidene-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

: 942622-22-2
6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / hydrogen chloride; methanol / 2 h / 20 °C

2: 83 percent / pyridine / 0.5 h / 20 °C

3: 57 percent / N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate; MS 4 Angstroem / CH₂Cl₂ / 1 h / -40 °C

4: 98 percent / pyridine / 4 h / 20 °C

With pyridine; hydrogenchloride; methanol; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; MS 4 Angstroem; In dichloromethane;
DOI:10.1016/j.tetlet.2007.03.138

Reference yield:

: 3'-O-benzoyl-3-O-methoxymethyl-4',6'-O-tetraisopropyldisiloxanilidene sucrose

: 942622-22-2
6,1'-di-O-acetyl-4,3'-di-O-benzoyl-3-O-methoxymethyl-2-O-(3,4,6-tri-O-methoxymethyl-2-O-N-phenylcarbamoyl-β-D-glucopyranosyl)-4',6'-O-tetraisopropyldisiloxanilidene sucrose

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / pyridine / 0.5 h / 20 °C

2: 57 percent / N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate; MS 4 Angstroem / CH₂Cl₂ / 1 h / -40 °C

3: 98 percent / pyridine / 4 h / 20 °C

With pyridine; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; MS 4 Angstroem; In dichloromethane;
DOI:10.1016/j.tetlet.2007.03.138