2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

Base Information

Chemical Name:2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl
CAS No.:63107-92-6
Molecular Formula:C₂₄H₂F₁₆
Molecular Weight:594.254
Hs Code.:

Synonyms:2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

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Chemical Property of 2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

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Technology Process of 2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

There total 3 articles about 2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1559-88-2
1-bromo-2,3,5,6-tetrafluorobenzene

: 10386-84-2
4,4'-dibromo-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl

: 63107-92-6
2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

Guidance literature:: 1-bromo-2,3,5,6-tetrafluorobenzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 1h;

With copper(I) bromide; In tetrahydrofuran; 1,4-dioxane; at 20 ℃;

4,4'-dibromo-2,3,5,6,2',3',5',6'-octafluoro-1,1'-biphenyl; In tetrahydrofuran; 1,4-dioxane; toluene; at 110 ℃; for 72h; Further stages.;
DOI:10.1021/ja002309o

Reference yield:

: 392-57-4
1,4-diiodo-2,3,5,6-tetrafluorobenzene

: 3883-86-1
2,2',3,3',5,5',6,6'-octafluoro-1,1'-biphenyl

: 63107-91-5
2,2′,2″,3,3′,3″,5,5′,5″,6,6′,6″-dodecafluoro-1,1′:4′,1″-terphenyl

: 63107-92-6
2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

: 2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6''',2'''',3'''',5'''',6''''-eicosafluoro-<1,1';4',1'';4'',1''';4''',1''''>-quinquephenyl

Guidance literature:: With 1-methyl-pyrrolidin-2-one; lithium aluminium tetrahydride; copper(I) thiophene-2-carboxylate; Yields of byproduct given; 1.) NMP, room temperature, 96 h, 2.) ether, THF, 0 deg C, 1 h.;
DOI:10.1016/S0040-4020(98)00919-3

Reference yield:

: 327-54-8
1,2,4,5-Tetrafluorobenzene

: 63107-92-6
2,3,5,6,2',3',5',6',2'',3'',5'',6'',2''',3''',5''',6'''-hexadecafluoro-<1,1';4',1'';4'',1'''>-quaterphenyl

Guidance literature:: 1,2,4,5-Tetrafluorobenzene; With Pd⁽¹¹¹⁾; at 160 ℃; for 0.25h; under 7.50075E-10 Torr;

at 200 ℃; for 0.25h;
DOI:10.1039/c7cc01476g