C₄₃H₃₁N₃O₆S₃

Base Information

• Chemical Name: C₄₃H₃₁N₃O₆S₃
• CAS No.: 115127-32-7
• Molecular Formula: C₄₃H₃₁N₃O₆S₃
• Molecular Weight: 781.934
• Mol file: 115127-32-7.mol

Synonyms:C₄₃H₃₁N₃O₆S₃

Chemical Property of C₄₃H₃₁N₃O₆S₃

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₄₃H₃₁N₃O₆S₃

There total 2 articles about C₄₃H₃₁N₃O₆S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-chloro-1,3-dithiane (57529-04-1) + 1-(phenylsulfonyl)-2-(trimethylsilyl)-1H-indole (115127-31-6) → C43H31N3O6S3 (115127-32-7)

Guidance literature:

With titanium tetrachloride; In dichloromethane; 0 deg C 30 min, reflux 4 h, R_.T_. overnight;

DOI:10.1016/S0040-4020(01)85835-X

Reference yield:

1-benzenesulfonylindole (40899-71-6) → C43H31N3O6S3 (115127-32-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) tert-butyllithium / 1.) THF, -10 deg C, 45 min; 2.) THF, -20 deg C, 2 h

2: 65 percent / TiCl₄ / CH₂Cl₂ / 0 deg C 30 min, reflux 4 h, R_.T_. overnight

With tert.-butyl lithium; titanium tetrachloride; In dichloromethane;

DOI:10.1016/S0040-4020(01)85835-X

upstream raw materials:

2-chloro-1,3-dithiane

1-(phenylsulfonyl)-2-(trimethylsilyl)-1H-indole

1-benzenesulfonylindole

Refernces