4,4'-diisopropyl-deoxybenzoin

Base Information

• Chemical Name: 4,4'-diisopropyl-deoxybenzoin
• CAS No.: 79135-61-8
• Molecular Formula: C₂₀H₂₄O
• Molecular Weight: 280.41
• Mol file: 79135-61-8.mol

Synonyms:4,4'-diisopropyl-deoxybenzoin

Chemical Property of 4,4'-diisopropyl-deoxybenzoin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-diisopropyl-deoxybenzoin

There total 8 articles about 4,4'-diisopropyl-deoxybenzoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-isopropylbenzaldehyde) (122-03-2) → (E)-1,2-bis(4-isopropylphenyl)ethene (37163-82-9) + Bis-p-isopropylphenyl-acetaldehyd + 4,4'-diisopropyl-deoxybenzoin (79135-61-8)

Guidance literature:

With H₅PV₂Mo₁₀O₄₀(1,11); hydrogen; Pt(N-(2,6-diisopropylphenyl)pyrazin-2-ylmethanimine)Cl₂; at 100 ℃; for 18h; under 1900.13 Torr; Title compound not separated from byproducts.;

DOI:10.1039/b710100g

Reference yield:

4,4'-diisopropylbenzoin (5623-24-5) → 4,4'-diisopropyl-deoxybenzoin (79135-61-8)

Guidance literature:

With hydrogenchloride; amalgamated tin; In ethanol; for 72h; Yield given; Heating;

DOI:10.1021/jo00336a013

Reference yield:

1,2-bis(4-isopropylphenyl)acetylene (79135-52-7) → 4,4'-diisopropyl-deoxybenzoin (79135-61-8)

Guidance literature:

With sulfuric acid; water; In acetic acid; Yield given; 1.) reflux, 20 min, 2.) reflux, 2 h;

DOI:10.1021/jo00336a013

upstream raw materials:

(4-isopropylbenzaldehyde)

4,4'-diisopropylbenzoin

1,2-bis(4-isopropylphenyl)acetylene

hydrogenchloride

Refernces

• 1、 Han, G. Y.,Han, P. F.,Perkins, J.,McBay, H. C.. "Hydrogenation Reactions of Some Spool-Shaped Acetylenes". . p. 4695 - 4700. Retrieved 2007/10/02.