(E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

Base Information

Chemical Name:(E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide
CAS No.:1257305-53-5
Molecular Formula:C₂₈H₄₁NO₈
Molecular Weight:519.635
Hs Code.:

Synonyms:(E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

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Chemical Property of (E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

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Technology Process of (E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

There total 1 articles about (E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1257305-52-4
(E)-ethyl 4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-enoate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1257305-53-5
(E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

Guidance literature:: With isopropylmagnesium chloride; In tetrahydrofuran; at -25 - 0 ℃; for 0.75h;
DOI:10.1021/ol102468k

Reference yield: 91.0%

: 1257305-53-5
(E)-4-((4S,5S)-5-((S)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-ynyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

: 1257305-49-9
(E)-4-((4S,5S)-5-((5S,Z)-1-(ethoxymethoxy)-5-(4-methoxybenzyloxy)hex-2-enyl)-2,2-dimethyl-1,3-dioxolan-4-yl)-N-methoxy-N-methylbut-2-enamide

Guidance literature:: With quinoline; hydrogen; In ethyl acetate; for 2h; under 760.051 Torr; optical yield given as %de;
DOI:10.1021/ol102468k