7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid

Base Information

• Chemical Name: 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid
• CAS No.: 93362-80-2
• Molecular Formula: C₂₇H₃₁NO₃S
• Molecular Weight: 449.614

Synonyms:7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid

Chemical Property of 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid

Chemical Property:

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Technology Process of 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid

There total 2 articles about 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-(cyclohex-1-en-1-yl)piperidine (2981-10-4) + 3-Benzyliden-2,3-dihydro-4H-1-benzothiopyran-4-on-1,1-dioxid (101001-24-5) → 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid (93362-80-2)

Guidance literature:

In methanol; for 0.5h; Ambient temperature;

DOI:10.1002/ardp.19843171010

Reference yield:

Z-3-benzylidene-1-thiochromanone (74074-09-2) → 7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid (93362-80-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / 30percent H₂O₂ / acetic acid / 1 h / Heating

2: 98 percent / methanol / 0.5 h / Ambient temperature

With dihydrogen peroxide; In methanol; acetic acid;

DOI:10.1002/ardp.19843171010

Reference yield: 71.0%

7,7a,8,9,10,11-Hexahydro-7-phenyl-11a-piperidino-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid (93362-80-2) → 7,7a,8,9,10,11-Hexahydro-7-phenyl-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-11a-ol-5,5-dioxid (93362-83-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 5.5h; Heating;

DOI:10.1002/ardp.19843171010

upstream raw materials:

1-(cyclohex-1-en-1-yl)piperidine

3-Benzyliden-2,3-dihydro-4H-1-benzothiopyran-4-on-1,1-dioxid

Z-3-benzylidene-1-thiochromanone

Downstream raw materials:

7,7a,8,9,10,11-Hexahydro-7-phenyl-6H,11aH-<1>benzothiopyrano<4,3-b>chromen-11a-ol-5,5-dioxid

8,9,10,11-Tetrahydro-7-phenyl-6H,7H-<1>benzothiopyrano<4,3-b>chromen-5,5-dioxid

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