dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

Base Information

Chemical Name:dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate
CAS No.:1207379-15-4
Molecular Formula:C₁₇H₁₉N₃O₄S
Molecular Weight:361.422
Hs Code.:

Synonyms:dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

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Chemical Property of dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

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Technology Process of dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

There total 2 articles about dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 762-42-5
dimethyl acetylenedicarboxylate

: 191349-02-7
1,3-dihydro-4,5-dimethyl-1-(phenylamino)-2H-imidazole-2-thione

: 1207379-15-4
dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

Guidance literature:: 1,3-dihydro-4,5-dimethyl-1-(phenylamino)-2H-imidazole-2-thione; With methanol; sodium; at 20 ℃;

dimethyl acetylenedicarboxylate; In methanol; at 20 ℃; for 4h;

With water; In methanol; Cooling with ice;
DOI:10.1016/j.tet.2009.11.056

Reference yield:

: dimethyl 2-[(1-anilino-4,5-dimethyl-1H-imidazol-2-yl)thio]but-2-enedioate

: 1207379-16-5
dimethyl (2Z)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

: 1207379-15-4
dimethyl (2E)-2-[4,5-dimethyl-2-thioxo-2,3-dihydro-1H-imidazol-1-yl(phenyl)amino]but-2-enedioate

Guidance literature:: dimethyl 2-[(1-anilino-4,5-dimethyl-1H-imidazol-2-yl)thio]but-2-enedioate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 3h; Inert atmosphere;

With water; In tetrahydrofuran; mineral oil; optical yield given as %de; Cooling with ice;
DOI:10.1016/j.tet.2009.11.056