9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

Base Information

Chemical Name:9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol
CAS No.:143076-86-2
Molecular Formula:C₂₄H₂₈N₂O₂
Molecular Weight:376.499
Hs Code.:

Synonyms:9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

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Chemical Property of 9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

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Technology Process of 9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

There total 6 articles about 9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 107-21-1
ethylene glycol

: 143076-85-1
3-(9-Benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propanal

: 143076-86-2
9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

Guidance literature:: With 4 A molecular sieve; toluene-4-sulfonic acid; In chloroform; for 24h; Heating;

Reference yield:

: 100-39-0
benzyl bromide

: 143076-86-2
9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH / 1) DMSO, r. t., 1h , 2) DMSO, r. t.

2: 78 percent / conc. H₂SO₄ / 5 h / Heating

3: 67 percent / diisobutylaluminumhydride / CH₂Cl₂ / -80 °C

4: 97 percent / p-toluenesulfonic acid, molecular sieves (4 Angstroem) / CHCl₃ / 24 h / Heating

With 4 A molecular sieve; sulfuric acid; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In dichloromethane; chloroform;

Reference yield:

: 143076-82-8
3-(2-Methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionsaeure

: 143076-86-2
9-Benzyl-1-<2-(1,3-dioxolan-2-yl)ethyl>-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol

Guidance literature:: Multi-step reaction with 4 steps

1: 1) NaH / 1) DMSO, r. t., 1h , 2) DMSO, r. t.

2: 78 percent / conc. H₂SO₄ / 5 h / Heating

3: 67 percent / diisobutylaluminumhydride / CH₂Cl₂ / -80 °C

4: 97 percent / p-toluenesulfonic acid, molecular sieves (4 Angstroem) / CHCl₃ / 24 h / Heating

With 4 A molecular sieve; sulfuric acid; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In dichloromethane; chloroform;